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- Nine samples of the patina and three samples of the rock, were examined
using stereoscopic microscopy, Scanning Electron Microscopy (SEM)
equipped with Energy Dispersive Spectrometer (EDS), X-ray diffraction
(XRD) and inductively coupled plasma atomic emission spectroscopy
(ICP-AES).
- The patina samples are composed of Si, O, Ca, Al, Mg, K and Fe. They contain angular carbon particles
and an anomalous amount of globules of pure gold, each about 1 µm in
size. The patina is enriched relatively to the rock by about 12% Fe2O3
and 4% CaO, and diluted in K and Al.
- No evidence was found that could indicate the addition, adhesion or
dispersion of artificial patina (or natural patina from a different
stone) to the plate or the letters.
- The rock is black, fine-textured, well-bedded arkosic sandstone
comprised mainly of silt-sized minerals with the addition of some quartz
grains up to 0.5 mm in size. It was identified as originating from the
Cambrian Shehoret Formation of southern Israel and Sinai, or its
equivalent beds east of the Dead Sea and the eastern Arabah Valley.
- The carbon particles from within the patina were subjected for AMS
radiocarbon age determination. The conventional radiocarbon age was
2250±40 BP (2-Sigma calibrated result: 390-200 BCE).
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